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Beilstein J. Org. Chem. 2011, 7, 1441–1448, doi:10.3762/bjoc.7.168
Graphical Abstract
Scheme 1: Hassner's synthesis of vinyl azides and a stable, nonexplosive analogue 5 of iodine azide (1).
Scheme 2: Preparation of polymer-bound bisazido iodate(I) 5 and polymer-bound 1,8-diaza-[5.4.0]bicyclo-7-unde...
Scheme 3: Two-step protocol for the preparation of vinyl azides 4a–e and 4g–i under flow conditions.
Scheme 4: Regeneration of functionalized polymers 5 and 8.
Scheme 5: Preparation of triazoles 12a–l by using inductively heated copper turnings as a packed-bed material...